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Analysis of Whirling of Gas Flow within the Specimen Chamber of ESEM
Bayer, Robert
The usage of an Environmental scanning electron microscope (ESEM) brings the possibility of studying many kinds of materials and chemical reactions never studied before. In this article there are compared and analyzed several simulation results of gas flow in the specimen chamber of ESEM with high gas pressure throughout the whole volume except on its optical axis, where low gas pressure is needed.
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The effect of the shape of the intake ports for pumping in a Scintillation detector.
Flídr, Karel ; Vyroubal, Petr (referee) ; Maxa, Jiří (advisor)
The thesis is concerned with the design of the shape of suction canals used for pumping in the scintillation detector. The goal is to perform analysis of the model of the detector according to the current conception and then perform an optimalisation of the suction canals as per demands to their function. In the beginning of the thesis the history of the microscope and electron microscopy is described. The next chapter is focused on a more detailed description of ESEM. The following charter is dedicated to describing the scintillation detector.The thesis recounts the kinds of liquid flow. In conclusion the programs SolidWorks and Ansys Fleunt are described. Next part of this thesis describes in detail parameters‘ settings of simulation calculation. Following chapter introduces designed changes of suction channels shape and its results are shown and described.
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Analysis of the gas flow in the passage of the primary electron beam differentially pumped chamber depending on the shape of the nozzle inlet
Hladký, David ; Vaculík, Sebastian (referee) ; Maxa, Jiří (advisor)
It is necessary to separate sample chamber with pressure up to 2000 Pa and the surroundings of tube with pressure 0.01 Pa with help of a differential pumped chamber at the environmental scanning electron microscope This differential pumped chamber is to be designed so that it has to manage to separate sections with very different pressures sufficiently and in the trajectory of transitting (overflying) prime electrons the average value of pressure and density has to be as low as possible, so that it would occure the lowest diffusion of these electrons, which is caused by collisions of electrons and air molecules too. It were created axisymmetric 2D models variant of Differentially pumped chamber with different opening angles of the clone, which were analyzed to choose the best variant. The Ansys Fluent systeme using finite volume method for analysis of fluid flow was used for analysis.
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Comparison of flow conditions in the gas detector used in the aperture and screen
Hubáček, Jiří ; Špinka, Jiří (referee) ; Maxa, Jiří (advisor)
The first part of the thesis deals with electron microscopy and physical model fluid flow. In the next part, a three-dimensional model is created in programme SolidWorks. It is the model of scintilating detector with aperture or screen with three hundred little apertures. These models are submitted to analysis focusing on investigation of the gas flow at different pressure in chamber of specimen ESEM using Cosmos FloWorks system. The results of the analysis of both apertures variants are compared with the request to minimize the pressure in the trajectory of the secondary electrons as well as in the chamber of specimen.
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Construction scintillation detector with one aperture for environmental scanning electron microscope
Přichystal, Vít ; Vyroubal, Petr (referee) ; Maxa, Jiří (advisor)
The thesis is focused on the design of a scintillation detector with one screen for environmental scanning electron microscope. At the beginning of the work is an introduction to microscopy. Further work is focused on the description of ESEM microscope and a scintillation detector. The following chapter is devoted to the dynamics of flow. They list the types of flow and mathematical description of equations. The next chapter is about using the software and the way of solution of flow. In the following chapter describes a proposal of the diaphragm and extraction method of the detector area. They are described some of type aperture. The last chapter is the conclusion, where the work is summarized.
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FLOW ANALYSIS OF THE PRESSURE IN THE EXPERIMENTAL CHAMBER OF THE DIFFERENTIAL PUMPING
Šabacká, Pavla ; Bílek, Michal (referee) ; Maxa, Jiří (advisor)
The thesis deals with the effect of the critical flow, which is produced at pumping of the differential pumping chamber of the Environmental Scanning Electron Microscope (ESEM). The thesis compares the state of the flow in the area of pumped chamber at pressure ratio on the apertures when the critical flow occurs and its advantages in design of the chambers versus the flow without the clogging the nozzle. Problematics were solved using finite volume method by Ansys Fluent system.
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Nanofibrous Separators for Lithium-Ion Batteries
Pléha, David ; Míka, Martin (referee) ; Janderka,, Pavel (referee) ; Novák, Vítězslav (advisor)
Nanofibrous separators use in lithium-ion batteries brings many advantages. In contrast to contemporary used commercial separators, nanofibrous ones exhibit higher temperature resistance,ionic conductivity and higher electrolyte uptake. Better ionic conductivity is ensured by porous structure and large specific surface. Fibers creates channels for the ionic species motion. Amorphous texture of nanofibers allows quick lithium ionic species motion within the polymeric matrix of separator. Furthermore, these separators exhibit higher volume of uptaken electrolyte. Further advantage of electrospinned nanofibrous separators are both high porosity and chemical stability.
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Observation of Insulators in ESEM
Matějka, Milan ; Špinka, Jiří (referee) ; Jirák, Josef (advisor)
This graduation theses in introduction deals with principle and problems of electron signal detection in scanning electron microscopy and charging of insulating specimens in SEM. The experimental part of the thesis describe the methods of qualification and quantification of insulating specimen charging effect observed in environmental scanning electron microscope through the use of ionisation and scintillation detector in dependence on water vapour pressure in specimen chamber. The goal of the thesis is formation of the methodics useful to evaluate charging effect at insulating specimens observing and on the basis of measuring, determine optimal conditions for insulating specimen observation with ionisation and scintillation detector.
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Detection of signal electrons in ESEM
Šváb, Martin ; Špinka, Jiří (referee) ; Jirák, Josef (advisor)
This bachelor's thesis deals with problems of environmental scanning electron microscopy and with detection of signal electrons at higher pressure in working chamber. In this thesis I will focus on comparison of detected signal level achieved under different working conditions.
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